HRID464029

反应详情

EQUATION

反应方程式

HRID 464029 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Dissolve 10 g (0.055 mole) of 4-(4-chlorophenyl)but-2-yn-1-ol in 100 ml of acetone. Add 0.6 g of Lindlar's catalyst. Stir the mixture under 1 atmosphere of hydrogen at room temperature. Follow the progress of the reaction by NMR. At the completion of the reaction, filter to remove the catalyst and evaporate to yield the title compound.

WORKUP

后处理

  1. customthe progress of the reaction by NMR
  2. customAt the completion of the reaction
  3. filtrationfilter
  4. customto remove the catalyst
  5. customevaporate