HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Chlorophenyl)but-2-yn-1-ol → HCID 13660260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Chlorophenyl)but-2-yn-1-ol | HCID 13660258 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Lindlars catalyst | HCID 131709914 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 13660260 | HCID 13660260 | — |
Reaction Steps
Dissolve 10 g (0.055 mole) of 4-(4-chlorophenyl)but-2-yn-1-ol in 100 ml of acetone. Add 0.6 g of Lindlar's catalyst. Stir the mixture under 1 atmosphere of hydrogen at room temperature. Follow the progress of the reaction by NMR. At the completion of the reaction, filter to remove the catalyst and evaporate to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04545995 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-e9db3053a42a47aca4797f058a311f27 |
| Source note | uspto-grants-1985_10 |