HRID464035

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID12496130

N,N-Diethylheptan-1-amine

C11H25N

$反应SMILES：Cc1ccc(S(=O)(=O)[O-])cc1.OC/C=C\Cc1ccc(Cl)cc1$

HCID131714350

未命名化合物

PRODUCTS

产物

$反应SMILES：CCCCCCC[N+](CC)(CC)C/C=C\Cc1ccc(Cl)cc1.Cc1ccc(S(=O)(=O)[O-])cc1$

HCID13660242

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

Mix 5.40 g (0.016 mole) of (Z)-4-(4-chlorophenyl)but-2-en-1-ol 4-methylbenzenesulfonate and 10.96 g (0.064 mole) of N,N-diethylheptanamine in 200 ml of acetonitrile. Stir the mixture at room temperature for 2 hours. Evaporate and recrystallize from ethyl acetate to yield the title compound, m.p. 79°-80° C.

WORKUP

后处理

customEvaporate
customrecrystallize from ethyl acetate