HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Diethyl-1-heptanamine → (Z)-4-(4-Chlorophenyl)-N,N-diethyl-N-heptyl-2-buten-1-aminium 4-methylbenzenesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Diethyl-1-heptanamine | HCID 12496130 | — |
| Reactant | (Z)-4-(4-Chlorophenyl)-2-buten-1-ol 4-methylbenzenesulfonate | HCID 131714350 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | (Z)-4-(4-Chlorophenyl)-N,N-diethyl-N-heptyl-2-buten-1-aminium 4-methylbenzenesulfonate | HCID 13660242 | — |
Reaction Steps
Mix 5.40 g (0.016 mole) of (Z)-4-(4-chlorophenyl)but-2-en-1-ol 4-methylbenzenesulfonate and 10.96 g (0.064 mole) of N,N-diethylheptanamine in 200 ml of acetonitrile. Stir the mixture at room temperature for 2 hours. Evaporate and recrystallize from ethyl acetate to yield the title compound, m.p. 79°-80° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04545995 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-2d2e8ee335394a5fb66d31299340c9f4 |
| Source note | uspto-grants-1985_10 |