Hydrochloric Acid → HCID 20263724, compound

HRID 464037Notes

Reaction equation

HRID 464037 reaction equation
[NH2:1][O:2][CH:3]([O:11][NH2:12])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[ClH:13]>>[ClH:13].[NH2:12][O:11][CH:3]([O:2][NH2:1])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 20263725HCID 20263725, compound

Product 1

HCID 20263724HCID 20263724, compound

Procedure

Under agitation, 16.43 g of diaminooxyoctane is combined with 167.3 ml of 1N aqueous hydrochloric acid until the pH of the solution is 2.4. The solution is then concentrated under vacuum and the residue recrystallized from 93% strength ethanol, thus obtaining 14.83 g of diaminooxyoctane monohydrochloride, mp 174° C.

Workup

  1. concentrationThe solution is then concentrated under vacuum
  2. customthe residue recrystallized from 93% strength ethanol

Sources & evidence

ORD record
ord-780f1f2ab4534798a424c8cd96d649e4
Source dataset
uspto-grants-1985_10
Patent number
US04546078

Reaction notes

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