反应详情

温度

84 °C

A solution of 99.66 g of triphenylphosphine and 37.82 g of chloromethyl ethyl ether in 240 ml of dry benzene was stirred and refluxed (84° C.) for 6 hours. The mixture then was chilled and filtered to give 7, as a white solid, mp 205°-206° C.

1. temperatureThe mixture then was chilled
2. filtrationfiltered
3. customto give 7