HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 1,4-bis(Vinylsulfonyl)-2,3-butanediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1,4-Bis(2-chloroethanesulfonyl)butane-2,3-diol | HCID 13469204 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1,4-bis(Vinylsulfonyl)-2,3-butanediol | HCID 20387005 | 84.7% |
Reaction Steps
11.4 g of 1,4-bis(chloroethylsulfonyl)-2,3-butanediol was dissolved in 300 ml of acetone and the same procedures as described in Synthesis Example 3 were followed using 6.8 g of triethylamine to obtain 7.6 g of white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04173481 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-8e10c8cdf612462abec5054ea2b41cc5 |
| Source note | uspto-grants-1979_11 |