HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 464110Generated: October 30, 2026
Sodium Hydroxide → Azobisisobutyronitrile
https://huagongshe.com/reaction/464110
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Amino-2-methylpropionitrile | HCID 88022 | — |
| Catalyst | Hexadecyltrimethylammonium chloride | HCID 8154 | — |
| Product | Azobisisobutyronitrile | HCID 6547 | 96% |
Reaction Steps
3 ml of `Arquad 16-29` is added, followed by 2.2 equivalents of caustic soda. While maintaining the temperature at 20° C., 26 mg of 2-amino-2-methyl-propanenitrile is added over 20 minutes and the title compound is isolated as in Example 1. Yield 96%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04546174 |
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| Source dataset | uspto-grants-1985_10 |
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| ORD ID | ord-2477a7439aed43528a1ce2062e84846d |
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| Source note | uspto-grants-1985_10 |
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