HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl orthoacetate → HCID 20264252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl orthoacetate | HCID 66221 | — |
| Reactant | HCID 1492084 | HCID 1492084 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 20264252 | HCID 20264252 | — |
Reaction Steps
A 3.0 g portion of 3-amino-2-hydrazino-6-methyl-4(3H)-pyrimidinone, 20 ml of triethyl orthoacetate and 100 ml of n-butanol was reacted as described in Example 1, giving 2.36 g of the desired intermediate, mp 287°-289° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04546181 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-9a6c81b042c34e96afb10916fe5a20f7 |
| Source note | uspto-grants-1985_10 |