Benzene, (triethoxymethyl)- → HCID 20264247, compound

HRID 464120Notes

Reaction equation

HRID 464120 reaction equation
[NH2:1][N:2]1[C:7](=[O:8])[CH:6]=[C:5]([CH3:9])[N:4]=[C:3]1[NH:10][NH2:11].CCO[C:15](OCC)(OCC)[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>C(O)CCC>[NH2:11][N:10]1[C:3]2=[N:4][C:5]([CH3:9])=[CH:6][C:7](=[O:8])[N:2]2[N:1]=[C:15]1[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

4

Reactant 2

HCID 74268Benzene, (triethoxymethyl)-HCID 1492084HCID 1492084, compound

Product 1

HCID 20264247HCID 20264247, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

A mixture of 2.0 g of 3-amino-2-hydrazino-6-methyl-4(3H)-pyrimidinone, 10 ml of triethyl orthobenzoate and 20 ml of n-butanol was reacted as described in Example 1, giving 1.27 g of the desired intermediate, mp 195° C. (dec.).

Workup

  1. customwas reacted

Sources & evidence

ORD record
ord-7cf8a23be58c4307b57a7196fc22937d
Source dataset
uspto-grants-1985_10
Patent number
US04546181

Reaction notes

Loading…