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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 464120Generated: October 30, 2026

Benzene, (triethoxymethyl)- → HCID 20264247, compound

https://huagongshe.com/reaction/464120

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzene, (triethoxymethyl)-HCID 74268—
ReactantHCID 1492084HCID 1492084—
Solvent1-ButanolHCID 263—
ProductHCID 20264247HCID 20264247—

Reaction Steps

A mixture of 2.0 g of 3-amino-2-hydrazino-6-methyl-4(3H)-pyrimidinone, 10 ml of triethyl orthobenzoate and 20 ml of n-butanol was reacted as described in Example 1, giving 1.27 g of the desired intermediate, mp 195° C. (dec.).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04546181
Source datasetuspto-grants-1985_10
ORD IDord-7cf8a23be58c4307b57a7196fc22937d
Source noteuspto-grants-1985_10