HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Ethyl 2-(6-chloro-3-nitro-2-pyridinyl)oxypropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 2-bromopropionate | HCID 79040 | — |
| Reactant | HCID 178526634 | HCID 178526634 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | Ethyl 2-(6-chloro-3-nitro-2-pyridinyl)oxypropanoate | HCID 13245757 | — |
Reaction Steps
A mixture of 8.8 grams of 3-nitro-6-chloro-2-pyridinol, 9 grams of ethyl α-bromopropionate and 6 grams of potassium carbonate was stirred in 50 ml of DMSO (dimethylsulfoxide) at ambient temperature for approximately 48 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04547218 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-c371f7fa04f6410a9daf14678034b5f7 |
| Source note | uspto-grants-1985_10 |