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HRID464228

反应详情

EQUATION

反应方程式

HRID 464228 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CCOC(=O)C(C)Br
HCID79040

Propanoic acid, 2-bromo-, ethyl ester

C5H9BrO2

结构：O=[N+]([O-])c1ccc(Cl)nc1O
HCID178526634

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)C(C)Oc1nc(Cl)ccc1[N+](=O)[O-]
HCID13245757

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

A mixture of 8.8 grams of 3-nitro-6-chloro-2-pyridinol, 9 grams of ethyl α-bromopropionate and 6 grams of potassium carbonate was stirred in 50 ml of DMSO (dimethylsulfoxide) at ambient temperature for approximately 48 hours.