HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Phenylethyl-2-methylthio-4-pyrimidone → HCID 20262871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Phenylethyl-2-methylthio-4-pyrimidone | HCID 12951508 | — |
| Reactant | N~1~-Methyl-N~1~-(pyridin-2-yl)propane-1,3-diamine | HCID 20262876 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 20262871 | HCID 20262871 | — |
Reaction Steps
2-[N-(3-aminopropyl)-N-methylamino]pyridine (0.81 g) and 2-methylthio-5-phenylethylpyrimid-4-one (1.0 g) were heated together under reflux in pyridine (2.5 ml) for 26 hr. After stripping, the residue was crystallised twice from ethanol and finally from acetone to give 2-[3-(N-methyl-N-pyrid-2-ylamino)propylamino]-5-phenylethylpyrimid-4-one, 0.68 g (46%) mp 134°-136° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04547506 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-c4a83da3c0ea43abaa72ad6767520951 |
| Source note | uspto-grants-1985_10 |