HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12951511, compound → HCID 53908143, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12951511 | HCID 12951511 | — |
| Reactant | N-(3-Aminopropyl)-N-methylpyridin-2-amine | HCID 20262876 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 53908143 | HCID 53908143 | — |
Reaction Steps
2-[N-(3-aminopropyl)-N-methylamino]pyridine (0.66 g) and 2-methylthio-5-(3,4-dichlorobenzyl)pyrimid-4-one (1.0 g) were heated together under reflux in pyridine (2.5 ml) for 24 hr. After stripping, the residue was recrystallised three times from ethanol/water to give 2-[3-(N-methyl-N-pyrid-2-ylamino)propylamino]-5-(3,4-dichlorobenzyl)pyrimid-4-one 0.25H2O, 1.0 g (70%) mp 104°-6° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04547506 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-a4bd19455e3c4eee8fb20c1d082183bb |
| Source note | uspto-grants-1985_10 |