HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophosgene → HCID 20262974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | HCID 20263068 | HCID 20263068 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 20262974 | HCID 20262974 | — |
Reaction Steps
3-(3,5-Dichlorophenoxy)pyrrolidine hydrochloride in a solvent mixture with excess tri-ethylamine is reacted with thiophosgene to give the title compound. The triethylamine hydrochloride by-product is removed by filtration and the product isolated by evaporating off excess solvent and triethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04547514 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-589e96f11b9747efaf6bb1b608ecd5f2 |
| Source note | uspto-grants-1985_10 |