HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Di-tert-butyl-4-mercaptophenol → Di-n-butyl 2-(3,5-di-tert-butyl-4-hydroxyphenylthio)succinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Reactant | Dibutyl maleate | HCID 5271569 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | Di-n-butyl 2-(3,5-di-tert-butyl-4-hydroxyphenylthio)succinate | HCID 20263298 | — |
Reaction Steps
The procedure of Example 1 is repeated using 11.92 grams of 2,6-di-tert-butyl-4-mercaptophenol, 11.41 grams of di-n-butyl maleate, and 0.5 gram of triethylamine. The product is purified by dry column chromatography to give a clear syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04547539 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-b2bc9e8de36f446db236c639b67b1d41 |
| Source note | uspto-grants-1985_10 |