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HRID464442

反应详情

EQUATION

反应方程式

HRID 464442 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)c1cc(S)cc(C(C)(C)C)c1O
HCID70370

2,6-Di-tert-butyl-4-mercaptophenol

C14H22OS

结构：CCCCOC(=O)/C=C\C(=O)OCCCC
HCID5271569

Dibutyl maleate

C12H20O4

PRODUCTS

生成物

1
结构：CCCCOC(=O)CC(Sc1cc(C(C)(C)C)c(O)c(C(C)(C)C)c1)C(=O)OCCCC
HCID20263298

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

The procedure of Example 1 is repeated using 11.92 grams of 2,6-di-tert-butyl-4-mercaptophenol, 11.41 grams of di-n-butyl maleate, and 0.5 gram of triethylamine. The product is purified by dry column chromatography to give a clear syrup.

WORKUP

后处理

  1. customThe product is purified
  2. customby dry column chromatography
  3. customto give a clear syrup