HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 2,3-Dihydro-1H-inden-1-one oxime
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 1-Indanone | HCID 6735 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2,3-Dihydro-1H-inden-1-one oxime | HCID 302323 | — |
Reaction Steps
A mixture of 1-indanone (100 g), hydroxylamine HCl (183 g), potassium carbonate (183 g), methanol (1700 ml) and water (170 ml) was heated at reflux for 18 hours, then cooled and poured into water. The title compound was filtered, washed with water and air-dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04548943 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-54390f6c62fb4669b8d72df83c6b7e0d |
| Source note | uspto-grants-1985_10 |