HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70481515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 20262497 | HCID 20262497 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70481515 | HCID 70481515 | — |
Reaction Steps
Excess 3% hydrogen chloride in methanol is added to a solution of 1.0 g 2-(p-methoxyphenethyl)-5-(2,2-dimethyl-1,3-benzoxathiol-5-yl)hydroxymethylpyrrolidine in 20 ml of methanol. Diethyl ether is added until precipitation is complete. 2-(p-methoxyphenethyl)-5-(2,2-dimethyl-1,3-benzoxathiol-5-yl)hydroxymethylpyrrolidine hydrochloride is filtered, washed with ether, air dried and recrystallized.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04548951 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-d09cb85c44b84c6696eaca2ff8fb556d |
| Source note | uspto-grants-1985_10 |