2-Chlorobenzoic Acid → HCID 20262575, compound

HRID 464795Notes

Reaction equation

HRID 464795 reaction equation
Cl[C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[CH2:11]([O:18][C:19]1[CH:20]=[C:21]([CH:23]=[CH:24][CH:25]=1)[NH2:22])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([O:18][C:19]1[CH:20]=[C:21]([NH:22][C:2]2[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=2[C:4]([OH:6])=[O:5])[CH:23]=[CH:24][CH:25]=1)[C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 83742-Chlorobenzoic AcidHCID 928923-Benzyloxyaniline

Product 1

HCID 20262575HCID 20262575, compound

Procedure

2-(3-Benzyloxyphenylamino)benzoic acid [VII; R and R"=H, OR°=3-OCH2C6H5 ] was prepared from 2-chlorobenzoic acid and 3-benzyloxyaniline according to the procedure of Example 1(a). The green solid obtained was used directly in the next reaction.

Workup

  1. customThe green solid obtained
  2. customwas used directly in the next reaction

Sources & evidence

ORD record
ord-61236eed7cf8404a91fa0ad62783dedc
Source dataset
uspto-grants-1985_10
Patent number
US04549016

Reaction notes

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