HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20262662, compound → HCID 20262669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20262662 | HCID 20262662 | — |
| Reactant | HCID 20262665 | HCID 20262665 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20262669 | HCID 20262669 | 94% |
Reaction Steps
Following the procedure of part (a) of Example I a 353.5 g sample of 2,4-dimethyl-2-(4-methylphenyl)-4-pentenal was reduced with 30 g of lithium aluminum hydride in 1100 ml of anhydrous ether. Usual workup and distillation afforded 335 g (94% yield) of the desired 2,4-dimethyl-2-(4-methylphenyl)-4-penten-1-ol (bp 136°-138° C./0.7 mm Hg) with a purity of 95%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04549029 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-3783fcfd63244ccdb9f27a4d0a36a391 |
| Source note | uspto-grants-1985_10 |