Hydrochloric Acid → HCID 23324062, compound

HRID 464821Notes

Reaction equation

HRID 464821 reaction equation
[CH2:1]([N:3]([CH2:25][CH3:26])[CH2:4][CH2:5][CH2:6][N:7]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[C:9]([NH:16][CH2:17][CH2:18][CH2:19][N:20]([CH2:23][CH3:24])[CH2:21][CH3:22])=[N:8]1)[CH3:2].[ClH:27].C(OCC)C>C(O)C>[ClH:27].[ClH:27].[CH2:25]([N:3]([CH2:1][CH3:2])[CH2:4][CH2:5][CH2:6][N:7]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[C:9]([NH:16][CH2:17][CH2:18][CH2:19][N:20]([CH2:21][CH3:22])[CH2:23][CH3:24])=[N:8]1)[CH3:26]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 30308371-(3-Diethylaminopropyl)-3-(3-diethylaminopropylamino)indazole

Product 1

HCID 23324062HCID 23324062, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

In 50 ml of absolute ethyl alcohol was dissolved 3.0 g of 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)indazole and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Anhydrous diethyl ether was added to the solution to separate crystals. Then the crystals were obtained by filtration and dried to give 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)indazole dihydrochloride.

Workup

  1. temperatureunder cooling with ice
  2. customto separate crystals
  3. customThen the crystals were obtained by filtration
  4. customdried

Sources & evidence

ORD record
ord-2518c1e06e92490b9665232195563ccf
Source dataset
uspto-grants-1985_10
Patent number
US04549023

Reaction notes

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