HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 3-(1,2-Dihydro-2-naphthalenyl)-1-methyl-2,5-pyrrolidinedione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Dihydro-3-(1,2-dihydro-2-naphthalenyl)-2,5-furandione | HCID 20387363 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-(1,2-Dihydro-2-naphthalenyl)-1-methyl-2,5-pyrrolidinedione | HCID 20387359 | — |
Reaction Steps
60 g of the above anhydride is added portionwise to a stirred 500 ml portion of aqueous methylamine. After addition is complete, the mixture is heated to boil off water and excess amine, ultimately to 210°-220° to complete the cyclization and form the title A compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04173640 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-4078e06ce38445eea78205e8999ebf4e |
| Source note | uspto-grants-1979_11 |