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HRID46500

反应详情

EQUATION

反应方程式

HRID 46500 的结构方程式

REACTANTS

反应物

2
结构：CN
HCID6329

Methylamine

CH5N

结构：O=C1CC(C2C=Cc3ccccc3C2)C(=O)O1
HCID20387363

未命名化合物

PRODUCTS

生成物

1
结构：CN1C(=O)CC(C2C=Cc3ccccc3C2)C1=O
HCID20387359

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

60 g of the above anhydride is added portionwise to a stirred 500 ml portion of aqueous methylamine. After addition is complete, the mixture is heated to boil off water and excess amine, ultimately to 210°-220° to complete the cyclization and form the title A compound.

WORKUP

后处理

  1. additionAfter addition
  2. temperaturethe mixture is heated
  3. customultimately to 210°-220°
  4. customform the title A compound