m-Chloroperbenzoic acid → HCID 13575684, compound

HRID 465029Notes

Reaction equation

HRID 465029 reaction equation
[CH3:1][O:2][C:3]([NH:5][NH:6][C:7]1[C:15]2[O:14][CH:13]([CH3:16])[CH2:12][C:11]=2[C:10]([CH3:17])=[C:9]([Cl:18])[CH:8]=1)=[O:4].C1C=C(Cl)C=C(C(OO)=O)C=1.COC(NNC1C2OC(C)CC=2C(C)=CC=1)=O>>[CH3:1][O:2][C:3]([N:5]=[N:6][C:7]1[C:15]2[O:14][CH:13]([CH3:16])[CH2:12][C:11]=2[C:10]([CH3:17])=[C:9]([Cl:18])[CH:8]=1)=[O:4]

Participants

4

Reactant 3

HCID 70297m-Chloroperbenzoic acidHCID 13575671HCID 13575671, compoundHCID 13575674HCID 13575674, compound

Product 1

HCID 13575684HCID 13575684, compound

Procedure

5 was prepared, as a red solid, m.p.: 112°-114° C., by treating 5A with MCPBA, according to the procedure described in Example 1 for preparing 1 from 1F.

Workup

  1. custom5 was prepared, as a red solid, m.p.: 112°-114° C.

Sources & evidence

ORD record
ord-8d30bfd235a340a984e21f63e895629f
Source dataset
uspto-grants-1985_10
Patent number
US04550121

Reaction notes

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