m-Chloroperbenzoic acid → HCID 53963307, compound

HRID 465030Notes

Reaction equation

HRID 465030 reaction equation
[CH3:1][O:2][C:3]([NH:5][NH:6][C:7]1[C:15]2[O:14][CH:13]([CH2:16][CH3:17])[CH2:12][C:11]=2[C:10]([CH3:18])=[CH:9][CH:8]=1)=[O:4].C1C=C(Cl)C=C(C(OO)=O)C=1.COC(NNC1C2OC(C)CC=2C(C)=CC=1)=O>>[CH3:1][O:2][C:3]([N:5]=[N:6][C:7]1[C:15]2[O:14][CH:13]([CH2:16][CH3:17])[CH2:12][C:11]=2[C:10]([CH3:18])=[CH:9][CH:8]=1)=[O:4]

Participants

4

Reactant 3

HCID 70297m-Chloroperbenzoic acidHCID 13575671HCID 13575671, compoundHCID 13575675HCID 13575675, compound

Product 1

HCID 53963307HCID 53963307, compound

Procedure

6 was prepared, as a red syrup by treating 6B with MCPBA, according to the procedure described in Example 1 for preparing 1 from 1F.

Workup

  1. custom6 was prepared, as a red syrup

Sources & evidence

ORD record
ord-84ffbfd3411a4c9fb1011282ff55cb3b
Source dataset
uspto-grants-1985_10
Patent number
US04550121

Reaction notes

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