Hydrogen Bromide → HCID 131714393, compound

Participants

Reaction Steps

The benzothiazole derivative (1 g) was subjected to reduction with lithium aluminum hydride (0.6 g) in anhydrous tetrahydrofuran (15 ml). Then, the product was refluxed by heating for 6 hrs in an aqueous solution (7.2 ml) of cystheamine hydrochloride (0.43 g) and 47% hydrobromide to yield 5-[(2-aminoethyl)thiomethyl]-2-dimethylaminomethylbenzothiazole.2hydrobromide (1.52 g).

Provenance & Evidence