HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-(Chloroacetyl)-5,11-dihydro-6H-pyrido(2,3-b)(1,4)benzodiazepin-6-one → HCID 178482789, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-(Chloroacetyl)-5,11-dihydro-6H-pyrido(2,3-b)(1,4)benzodiazepin-6-one | HCID 120053 | — |
| Reactant | HCID 178482790 | HCID 178482790 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178482789 | HCID 178482789 | — |
Reaction Steps
The title compound is prepared analogously to Example 2 from 11-(chloroacetyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and trans-2-[[(4-hydroxycyclohexyl)(methyl)-amino]methyl]piperidine to give colorless crystals, mp. 183°-184.5° C. (acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04550107 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-e62643dadd874beeaad0969a6a02298f |
| Source note | uspto-grants-1985_10 |