HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl-piperidin-3-ylmethyl-amine → HCID 20261521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl-piperidin-3-ylmethyl-amine | HCID 6484181 | — |
| Reactant | 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 10085419 | — |
| Solvent | Isopropanol ethyl acetate | HCID 22055037 | — |
| Product | HCID 20261521 | HCID 20261521 | — |
Reaction Steps
The title compound is prepared analogously to Example 35 from 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one and 3-[(diethylamino)methyl]piperidine to give colorless crystals, mp. 140° C. (isopropanol/ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04550107 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-435e844b91db4008a5738ff58e74d73f |
| Source note | uspto-grants-1985_10 |