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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 465086Generated: October 29, 2026

11-(Chloroacetyl)-5,11-dihydro-6H-pyrido(2,3-b)(1,4)benzodiazepin-6-one → HCID 20261509, compound

https://huagongshe.com/reaction/465086

Reaction equation

Participants

RoleNameHCIDCharge
Reactant11-(Chloroacetyl)-5,11-dihydro-6H-pyrido(2,3-b)(1,4)benzodiazepin-6-oneHCID 120053—
ReactantHCID 20261498HCID 20261498—
Solvent1-PropanolHCID 1031—
ProductHCID 20261509HCID 20261509—

Reaction Steps

The title compound is prepared analogously to Example 2 from 11-(chloroacetyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 3-(diethylamino)-hexahydro-1H-azepine to give colorless crystals, mp. 222°-224° C. (n-propanol).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04550107
Source datasetuspto-grants-1985_10
ORD IDord-1589409e1f444cab8c07572f45653d91
Source noteuspto-grants-1985_10