HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(1-Methylpyrrolidin-2-yl)piperidine → HCID 20261497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(1-Methylpyrrolidin-2-yl)piperidine | HCID 219458 | — |
| Reactant | 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 10085419 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 20261497 | HCID 20261497 | — |
Reaction Steps
The title compound is prepared analogously to Example 35 from 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one and hexahydronicotine to give colorless crystals, mp. 161°-163° C. (ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04550107 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-0bbdb77a847b48aebe2fd3b6a764db7c |
| Source note | uspto-grants-1985_10 |