HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one → 5,10-Dihydro-5-[[3-[(1-piperidinyl)methyl]-1-piperidinyl]-acetyl]-11H-dibenzo[b,e][1,4]diazepin-11-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 10085419 | — |
| Reactant | 1-[(Piperidin-3-yl)methyl]piperidine | HCID 12802904 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 5,10-Dihydro-5-[[3-[(1-piperidinyl)methyl]-1-piperidinyl]-acetyl]-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 20261530 | — |
Reaction Steps
The title compound is prepared analogously to Example 35 from 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one and 3-[(1-piperidinyl)methyl]piperidine to give colorless crystals, mp. 150°-152° C. (ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04550107 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-a57168feb90f49218ee060962f1bb584 |
| Source note | uspto-grants-1985_10 |