Hydrazine hydrate (1:1) → HCID 3571819, compound

HRID 465100Notes

Reaction equation

HRID 465100 reaction equation
CO[C:3]1[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][N:9]=1.O.[NH2:11][NH2:12]>C(O)C>[NH:11]([C:3]1[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][N:9]=1)[NH2:12]

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 756572H-Azepine, 3,4,5,6-tetrahydro-7-methoxy-

Product 1

HCID 3571819HCID 3571819, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A 22.5 g portion 7-methoxy-3,4,5,6-tetrahydro-2H-azepine was reacted with 11.3 g of hydrazine hydrate in 200 ml of ethanol by the procedure of Example 9, giving the desired intermediate.

Sources & evidence

ORD record
ord-1ce29b19d2184dce8ee2fd962a42327e
Source dataset
uspto-grants-1985_10
Patent number
US04550169

Reaction notes

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