Ammonia → HCID 20261960, compound

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Reaction Steps

Ammonia was led at room temperature for 28 hours into a solution of 11.7 g of the methyl 2-[N-{2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenyl}amino]propionate, obtained according to Example I, in 100 ml of methanol. After evaporating to dryness under reduced pressure and recrystallizing from acetonitrile, an orange crystalline substance was obtained having a melting-point of 187° C. Elementary analysis: 47.67% C (calculated 47.60), 3.24% H (calculated 3.25) and 10.24% N (calculated 10.41).

Provenance & Evidence