Oxalyl chloride → HCID 57120307, compound

HRID 465285Notes

Reaction equation

[CH3:1][C@@H:2]([CH2:6][CH2:7][C@@H:8]([O:10][CH2:11][CH2:12][CH3:13])[CH3:9])[C:3](O)=[O:4].C(Cl)(=O)C([Cl:17])=O>>[CH3:1][C@H:2]([CH2:6][CH2:7][C@@H:8]([O:10][CH2:11][CH2:12][CH3:13])[CH3:9])[C:3]([Cl:17])=[O:4]

Participants

Reactant 2

HCID 65578Oxalyl chloride

HCID 57248281HCID 57248281, compound

Product 1

HCID 57120307HCID 57120307, compound

Procedure

The (2S,5S)-2-methyl-5-propoxyhexanoic acid prepared above was reacted with oxalyl chloride to obtain (2R,5S)-2-methyl-5-propoxyhexanoic acid chloride. The title compound was prepared in the same manner as in Example 9 from the acid chloride obtained above and the corresponding core-compound, 4-octyloxyphenyl 4'-hydroxy-4-biphenylcarboxylate.

Sources & evidence

ORD record: ord-a9778b9c63f3466d9b3b0a3cadf76609
Source dataset: uspto-grants-1992_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05152919

Reaction notes

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