Hydrogen Peroxide → HCID 10086759, compound

Participants

Reaction Conditions

Reaction Steps

The carbonyl compound was prepared by combining 500 mg (1.7 mmol) of the quinoxaline compound (7) and 16 nil HOAc, and then adding 5 ml of 30% H2O2. The mixture was heated to 60° C. for 16 hours, and then cooled. The product was recovered by filtration and dried at 0.5 mm and 60° C. overnight, yielding 150 mg of 1-n-butyl-7,8-dichloro-1,2,4-triazolo[4,3-a]quinoxalin-4(5H)-one (8).

Provenance & Evidence