Hydrochloric Acid → HCID 70344612, compound

HRID 465352Notes

Reaction equation

HRID 465352 reaction equation
[CH2:1]([N:3]1[CH:7]=[C:6]([CH:8]=[CH:9][C:10]2[S:11][C:12]3[NH:13][CH2:14][CH2:15][CH2:16][C:17]=3[N:18]=2)[N:5]=[C:4]1[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[CH3:2].[ClH:25]>>[ClH:25].[ClH:25].[CH2:1]([N:3]1[CH:7]=[C:6]([CH:8]=[CH:9][C:10]2[S:11][C:12]3[NH:13][CH2:14][CH2:15][CH2:16][C:17]=3[N:18]=2)[N:5]=[C:4]1[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[CH3:2]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 53745361HCID 53745361, compound

Product 1

HCID 70344612HCID 70344612, compoundYield 94.2%

Procedure

2-{2-(1-Ethyl-2-phenylimidazol-4-yl)ethenyl}-4,5,6,7-tetrahydrothiazolo[5,4-b]pyridine was neutralized with hydrochloric acid and recrystallized from ethanoldiethyl ether to obtain the title compound (yield: 94.2%).

Workup

  1. customrecrystallized from ethanoldiethyl ether

Sources & evidence

ORD record
ord-7ea6ee1f157644adbcc03fcd488e5731
Source dataset
uspto-grants-1992_10
Patent number
US05153201

Reaction notes

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