HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic acid, 2-((4-chloro-2,5-dimethylphenyl)thio)- → 4-Chloro-2,5-dimethylbenzenethiol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic acid, 2-((4-chloro-2,5-dimethylphenyl)thio)- | HCID 66739 | — |
| Reactant | (4-t-Butylphenylthio)nitromethane | HCID 14404080 | — |
| Product | 4-Chloro-2,5-dimethylbenzenethiol | HCID 108862 | — |
Reaction Steps
The thioether (A) was obtained as an oil having a satisfactory NMR spectrum (200 MHz/CDCl3): 2.33 (s, 3H), 2.42 (s, 3H), 5.37 (s, 2H), 7.26 (s, 1H), 7.35 (s, 1H) from (4-chloro-2,5-dimethylphenylthio)aceti acid, itself obtained from 4-chloro-2,5-dimethylbenzenethiol, in both cases using analogous procedures to those described in Example 13.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05153227 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-68475e402ba547e0b6f162dbe8161876 |
| Source note | uspto-grants-1992_10 |