HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Hydroxybutyl)cyclohex-3-ene-1-one → 4-(4-Hydroxybutyl)cyclohexanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Hydroxybutyl)cyclohex-3-ene-1-one | HCID 10241195 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4-(4-Hydroxybutyl)cyclohexanone | HCID 10329738 | — |
Reaction Steps
To a solution of 4.63 g of 4-(4-hydroxybutyl)-cyclohex-3-ene-1-one in 130 ml acetone is added 0.46 g of 10% palladium on carbon and the suspension is then hydrogenated at 3 atmospheres (=3.04 bar) pressure for 3 h. The catalyst is evaporated to dryness to give 4-(4-hydroxybutyl)-cyclohexanone as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05153214 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-df360fff9976427c9665fb4cd578eb11 |
| Source note | uspto-grants-1992_10 |