HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N-[2-[[2,6-bis(1-Methylethyl)phenyl]amino]-2-oxoethyl]-N-(9H-fluoren-9-yl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 2-Methoxybenzoyl chloride | HCID 88969 | — |
| Reactant | N-[2,6-bis(1-Methylethyl)phenyl]-2-[(diphenylmethyl)amino]acetamide | HCID 1645639 | — |
| Product | N-[2-[[2,6-bis(1-Methylethyl)phenyl]amino]-2-oxoethyl]-N-(9H-fluoren-9-yl)benzamide | HCID 19874930 | — |
Reaction Steps
When in the procedure of Example 94 an appropriate amount of product of Example 77 was substituted for the product of Example 4 and an appropriate amount of benzoyl chloride was substituted for 2-methoxybenzoyl chloride and the general procedure of Example 94 was followed the title compound was obtained. Total yield, 0.56 g (76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05153226 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-1a15f7ce90fc4a2eb881c5192b494086 |
| Source note | uspto-grants-1992_10 |