HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178459181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-(p-Fluorobenzoyl)-3-methoxy-2-pentenonitrile | HCID 53800056 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178459181 | HCID 178459181 | — |
Reaction Steps
A two-phase mixture of 5.0 g. 2-(p-fluorobenzoyl)-3-methoxy-2-pentenonitrile in 50 ml. of chloroform is stirred with a 50 ml. solution of aqueous 1 N hydrochloric acid. After 24 hours, the organic phase is separated and evaporated. The residue is recrystallized from chloroform to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04173650 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-3fd7ec61b5f6425d86f700f94a3a5316 |
| Source note | uspto-grants-1979_11 |