HRID46568
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A two-phase mixture of 5.0 g. 2-(p-fluorobenzoyl)-3-methoxy-2-pentenonitrile in 50 ml. of chloroform is stirred with a 50 ml. solution of aqueous 1 N hydrochloric acid. After 24 hours, the organic phase is separated and evaporated. The residue is recrystallized from chloroform to yield the title compound.
WORKUP
后处理
- additionA two-phase mixture of 5.0 g
- customthe organic phase is separated
- customevaporated
- customThe residue is recrystallized from chloroform