HRID46568

反应详情

EQUATION

反应方程式

HRID 46568 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A two-phase mixture of 5.0 g. 2-(p-fluorobenzoyl)-3-methoxy-2-pentenonitrile in 50 ml. of chloroform is stirred with a 50 ml. solution of aqueous 1 N hydrochloric acid. After 24 hours, the organic phase is separated and evaporated. The residue is recrystallized from chloroform to yield the title compound.

WORKUP

后处理

  1. additionA two-phase mixture of 5.0 g
  2. customthe organic phase is separated
  3. customevaporated
  4. customThe residue is recrystallized from chloroform