Hydrochloric Acid → HCID 18648058, compound

HRID 465702Notes

Reaction equation

HRID 465702 reaction equation
C([O:3][CH:4]([O:12][CH2:13][CH3:14])[CH2:5][C:6](=[CH2:11])[C@H:7](O)[CH2:8][OH:9])C.Cl>>[CH2:13]([O:12][C@@H:4]1[O:3][C@H:7]([CH2:8][OH:9])[C:6](=[CH2:11])[CH2:5]1)[CH3:14].[CH2:13]([O:12][C@H:4]1[O:3][C@H:7]([CH2:8][OH:9])[C:6](=[CH2:11])[CH2:5]1)[CH3:14]

Participants

4

Procedure

reacting the product of step e with 10% HCl in a suitable solvent for 30 minutes to form (2S-cis)-tetrahydro-5-ethoxy-3-methylene-2-furanmethanol and (2S-trans)-tetrahydro-5-ethoxy-3-methylene-2-furanmethanol.

Workup

  1. customfor 30 minutes

Sources & evidence

ORD record
ord-c55d870f790446b4bd3545c60cb93e34
Source dataset
uspto-grants-1992_10
Patent number
US05153337

Reaction notes

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