Hydrochloric Acid → HCID 18648058, compound
Reaction equation
C([O:3][CH:4]([O:12][CH2:13][CH3:14])[CH2:5][C:6](=[CH2:11])[C@H:7](O)[CH2:8][OH:9])C.Cl>>[CH2:13]([O:12][C@@H:4]1[O:3][C@H:7]([CH2:8][OH:9])[C:6](=[CH2:11])[CH2:5]1)[CH3:14].[CH2:13]([O:12][C@H:4]1[O:3][C@H:7]([CH2:8][OH:9])[C:6](=[CH2:11])[CH2:5]1)[CH3:14]Participants
4
Procedure
reacting the product of step e with 10% HCl in a suitable solvent for 30 minutes to form (2S-cis)-tetrahydro-5-ethoxy-3-methylene-2-furanmethanol and (2S-trans)-tetrahydro-5-ethoxy-3-methylene-2-furanmethanol.
Workup
- customfor 30 minutes
Sources & evidence
- ORD record
- ord-c55d870f790446b4bd3545c60cb93e34
- Source dataset
- uspto-grants-1992_10
- Patent number
- US05153337
Reaction notes
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