1-Butanol → HCID 178450382, compound

Participants

Reaction Steps

The title compound was prepared in a manner analogous to the preparation of the compound of Example 11a, using 2-amino-6-chloropurine (Sigma, lot #69F4064, 4.4 g, 25.9 mmol) and sodium (Aldrich, lot #9621CL, 3 g, 129.5 mmol) in 250 mL n-butanol to give 4.4 g (21.2 mmol, 82%). mp=165° C.

Provenance & Evidence