HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 178508573, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 2-Amino-6-chloropurine | HCID 5360349 | — |
| Product | HCID 178508573 | HCID 178508573 | — |
Reaction Steps
2-Amino-6-chloropurine (Sigma, lot #69F4064, 5.0 g, 29.5 mmol) was stirred in pyrrolidine (Kodak, lot #B161, 30mL) at 80° C. for 24 hours. The solvent was evaporated to a gold solid which was recrystalized from methanol to yield 3.41 g (16.7 mmol, 58%); mp=265°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05153318 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-c79a1b2e75144d2d8ae55a4c5112e3d8 |
| Source note | uspto-grants-1992_10 |