N,N-Dimethyl-1,3-propanediamine → HCID 20386235, compound

HRID 46595Notes

Reaction equation

HRID 46595 reaction equation
[CH:1]1[C:6]([CH:7]=O)=[CH:5][C:4]2[O:9][CH2:10][O:11][C:3]=2[CH:2]=1.[CH3:12][N:13]([CH3:18])[CH2:14][CH2:15][CH2:16][NH2:17]>C1C=CC=CC=1>[CH3:12][N:13]([CH3:18])[CH2:14][CH2:15][CH2:16][N:17]=[CH:7][C:6]1[CH:1]=[CH:2][C:3]2[O:11][CH2:10][O:9][C:4]=2[CH:5]=1

Participants

4

Reactant 2

HCID 7993N,N-Dimethyl-1,3-propanediamineHCID 8438Piperonal

Product 1

HCID 20386235HCID 20386235, compoundYield 75.2%

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

Interaction of 50 g of piperonal and 34 g of 3-dimethylaminopropylamine in 240 ml. of benzene following the procedure described in Example 1 yields 58.6 g of the product as an oil, boiling point 131°-136° C. at 0.2-0.3 mm. of Hg.

Sources & evidence

ORD record
ord-fdac539c7ad5423f8cece9e11215f471
Source dataset
uspto-grants-1979_11
Patent number
US04174317

Reaction notes

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