HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethyl-1,3-propanediamine → HCID 20386235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Reactant | Piperonal | HCID 8438 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20386235 | HCID 20386235 | 75.2% |
Reaction Steps
Interaction of 50 g of piperonal and 34 g of 3-dimethylaminopropylamine in 240 ml. of benzene following the procedure described in Example 1 yields 58.6 g of the product as an oil, boiling point 131°-136° C. at 0.2-0.3 mm. of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04174317 |
| Source dataset | uspto-grants-1979_11 |
| ORD ID | ord-fdac539c7ad5423f8cece9e11215f471 |
| Source note | uspto-grants-1979_11 |