HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 15745425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 3-(2-Bromoethyl)oxazolo[4,5-b]pyridin-2(3H)-one | HCID 10377106 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15745425 | HCID 15745425 | — |
Reaction Steps
0.1 mol of isopropylamine and 0.01 mol of 3-(2-bromoethyl)-3H-oxazolo[4,5-b]pyridin-2-one, dissolved beforehand in 40 cm3 of acetonitrile, are introduced into a 100-cm3 ground-necked round-bottomed flask equipped with a reflux condenser. The mixture is heated to reflux for 15 hours. After cooling, the precipitate obtained is drained, dried and recrystallized.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05155116 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-7cfebfb08a1242a086cd6dc745ca372c |
| Source note | uspto-grants-1992_10 |