HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 15158150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 15158146 | HCID 15158146 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 15158150 | HCID 15158150 | 86% |
Reaction Steps
A concentrated hydrochloric acid (5 ml) was added to 3-(3-methoxypyridazin-4-yl)-2-phenylpyrazolo[1,5-a]pyridine (0.50 g) and refluxed for 2 hours and 30 minutes. After cooling, to the reaction mixture was added water (10 ml). The precipitates were collected by filtration to give 3-(3-oxo-2,3-dihydropyridazin-4-yl)-2-phenylpyrazolo[1,5-a]pyridine (0.41 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05155114 |
| Source dataset | uspto-grants-1992_10 |
| ORD ID | ord-4a35cc6bc94d47d68a810cd389e69dc0 |
| Source note | uspto-grants-1992_10 |